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Effect of hydrogen on the tensile strength of aged Ni-Ti superelastic alloy

Identifieur interne : 000106 ( France/Analysis ); précédent : 000105; suivant : 000107

Effect of hydrogen on the tensile strength of aged Ni-Ti superelastic alloy

Auteurs : Fehmi Gamaoun [Tunisie] ; Montassarbellah Ltaief [Tunisie] ; Tarak Bouraoui [Tunisie] ; Tarak Ben Zineb [France]

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RBID : Pascal:12-0043697

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Abstract

Because of its good corrosion resistance and biocompatibility, superelastic Ni-Ti wire alloys have been successfully used in orthodontic clinics. However, delayed fracture in the oral cavity has been observed. The susceptibility of a Ni-Ti shape-memory alloy toward hydrogen embrittlement has been examined with respect to the current densities and aging in air at room temperature. Orthodontic wires have been cathodically hydrogen charged using a different current density of 5, 10, and 20 A/m2 from 2 to 24 h in 0.9% NaCl aqueous solution at room temperature. The critical stress for the martensite transformation under a monotonous tensile test has been 20-90 MPa higher than that without hydrogen charging. In addition, embrittlement takes place in the austenite-martensite transformation plateau. For a short period of charging, the Ni-Ti alloy conserves its superelastic behavior. However, after 24 h of aging in air at room temperature, fracture at the austenite-martensite transformation plateau takes place earlier.


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<term>Cavité</term>
<term>Courant densité</term>
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<term>Alliage base nickel</term>
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<term>Fragilisation hydrogène</term>
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<div type="abstract" xml:lang="en">Because of its good corrosion resistance and biocompatibility, superelastic Ni-Ti wire alloys have been successfully used in orthodontic clinics. However, delayed fracture in the oral cavity has been observed. The susceptibility of a Ni-Ti shape-memory alloy toward hydrogen embrittlement has been examined with respect to the current densities and aging in air at room temperature. Orthodontic wires have been cathodically hydrogen charged using a different current density of 5, 10, and 20 A/m
<sup>2</sup>
from 2 to 24 h in 0.9% NaCl aqueous solution at room temperature. The critical stress for the martensite transformation under a monotonous tensile test has been 20-90 MPa higher than that without hydrogen charging. In addition, embrittlement takes place in the austenite-martensite transformation plateau. For a short period of charging, the Ni-Ti alloy conserves its superelastic behavior. However, after 24 h of aging in air at room temperature, fracture at the austenite-martensite transformation plateau takes place earlier.</div>
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